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apparatus and instruments for recording, transmitting, reproducing or processing sound, images or data; Sri, K. V. V., Anusha, A. & Sudhakar, M. UV-spectrophotometry method for the estimation of linagliptin in bulk and pharmaceutical formulations. Asian J. Res. Chem. 9(1), 47 (2016). Rajbangshi, J. C., Alam, M. M., Hossain, M. S., Islam, M. S. & Rouf, A. S. S. Development and validation of a RP-HPLC method for quantitative analysis of linagliptin in bulk and dosage forms. Dhaka Univ. J. Pharm. Sci. 17(2), 175–182 (2018). The TEGELI trademark was assigned an Application Number # UK00003730999 by the UK Intellectual Property Office (UKIPO). The researcher tested different volumes of HCI 37% (1–3mL), to select the appropriate acidic medium volume for LNG and PDAB reaction. The best results were obtained with 2mL of HCl 37% (Fig. 3c). Selection of temperature
apparatus and instruments for conducting, switching, transforming, accumulating, regulating or controlling the distribution or use of electricity; Sri, K. V., Anusha, M. & Reddy, S. R. A rapid RP-HPLC method development and validation for the analysis of linagliptinin bulk and pharmaceutical dosage form. Asian J. Pharm. Anal. 5(1), 16–20 (2015). Safe & Reliable: This type c charger is designed with double insulation protection and passed UKCA/CE Safety certified tests, safe to use and protect your device against over-voltage, over-current, over-heating, short-circuiting issues and ensures a safer and more stable charging for your usb-c device. Gurrala, S., Anumolu, P. D., Menkana, S., Gandla, N. & Toddi, K. Spectrophotometric estimation of linagliptin using ion-pair complexation and oxidative coupling reactions—a green approach. Thai J. Pharm. Sci. 44(4), 245–250 (2020).w/v): 1.25 g was dissolved in 25 mL of methanol with good shaking, and was freshly prepared. Analytical procedure Barapatre, S. R., Ganorkar, A. V. & Gupta, K. R. Quality by design-based HPLC assay method development and validation of linagliptin in tablet dosage form. Eur. J. Pharm. Med. Res. 4(02), 486–494 (2017). Preparation of ρDAB (2 × 10 –3mol/l) solution by dissolving 29.8mg in 100mL of methanol with good shaking, was freshly prepared. The effect of prolonged heating time on this reaction was controlled by monitoring the color development at different time intervals (10–60min) at 70–75°C. Maximum absorbance values were gained at 35min (Fig. 3b). Stability of the reaction product
Durga Anumolu, P. et al. Quantification of linagliptin by chemical derivatization with appliance of chromogenic. J. Appl. Chem. Res. 11(2), 39–50 (2017). Badugu, L. R. A validated RP-HPLC method for the determination of linagliptin. Am. J. Pharm. Tech. Res. 2(4), 463–470 (2012). The quantitative reaction rate was recorded by Job’s Method of Continuous Variations and the Molar ratio method 14. Mai, X. L. et al. A capillary electrophoresis method for the determination of the linagliptin enantiomeric impurity. J. Sep. Sci. 43(24), 4480–4487 (2020).Baink, S., Kaisar, M. M. & Hossain, M. S. Development and validation of a simple and rapid UV spectrophotometer method for assay of linagliptin in bulk and marketed dosage form. Indian J. Nov. Drug. Deliv. 5(4), 221–224 (2013).
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